A new
issue of this journal has just been published. To see abstracts of the papers
it contains (with links through to the full papers) click here:
Selected papers from the latest issue:
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2.
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Enrichment
of antioxidant compounds from lemon balm (Melissa officinalis) by
pressurized liquid extraction and enzyme-assisted extraction Original Research Article
Pages 1-9 T.L. Miron, M. Herrero, E. Ibáñez
Highlights
► EAE and
PLE are employed for the first time to obtain antioxidant compounds from
lemon balm. ► Enzyme treatment increases the extraction of total phenols and
antioxidant capacity of extracts. ► PLE allows extracting more efficiently
phenolic compounds from this sample. ► LC–MS/MS is employed to identify a
diverse group of phenolic compounds present on the extracts. |
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Column Liquid
Chromatography
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3.
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Rapid
detection of economic adulterants in fresh milk by liquid
chromatography–tandem mass spectrometry
Original Research
Article
Pages 10-20 Grant Abernethy, Kerianne Higgs
Highlights
► A rapid
LCMS means to spot 36 N-compounds that could be used to adulterate milk. ►
Biuret may be used as a marker for synthetic (fertilizer) urea adulteration
in milk. ► We threshold our interest to those levels where economic
adulteration is plausible. ► The method provides a presence/absence
indication for each analyte in ppm range. ► The method screens samples
abnormal by FTIR to reduce numbers sent to evidential tests. |
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4.
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Immunocapture
couples with matrix-assisted laser desorption/ionization time-of-flight mass
spectrometry for rapid detection of type 1 dengue virus Original Research Article
Pages 21-27 Wen-Hung Chen, I-Hsiang Hsu, Yuh-Chang Sun, Yu-Kuo Wang, Tung-Kung Wu
Highlights
►
Immunocapture coupled with MALDI-TOF MS method for DV1 detection was
developed. ► Detection limit of 105pfu/mL was low enough for early detection
of DF and DHF. ► Complex serum samples were tested to demonstrate the
feasibility of this method. |
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5.
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Impurities
preparation of sodium tanshinone IIA sulfonate by high-speed counter-current
chromatography and identification by liquid chromatography/multistage tandem
mass spectrometry Original Research Article
Pages 28-34 Shanqiao Chen, Xin Zhao, You Li, Dan Yang, Tingting Zhou, Guorong Fan
Highlights
► HSCCC
was applied in separating 3 related substances in low level from Sodium
Tanshinone IIA Sulfonate (STIIAS) bulk drug. ► Ammonium acetate was added
into the solvent system to inhibit the emulsification in separating
amphiphilic substances. ► The solvent system composed of
chloroform–n-butanol–methanol–water was established and optimized to
17:0.3:14:9. ► Seven compounds were enriched by HSCCC as pretreatment of
LC–MSn. To the best of our knowledge six compounds are first reported here. |
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6.
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Conical
coils counter-current chromatography for preparative isolation and
purification of tanshinones from Salvia miltiorrhiza Bunge Original Research Article
Pages 35-39 Junling Liang, Jie Meng, Mengzhe Guo, Zhi Yang, Shihua Wu
Highlights
► In this
work, we built a novel conical coil counter-current chromatography. ► The
conical coils were wound on the tapered holders, producing an extra gradient
centrifugal force. ► The gradient centrifugal force gradient was distributed
both in axial and radial directions. ► Thus it enabled CCC to retain more
stationary phase than conventional helical coils. ► By use of the conical
coil CCC, four tanshinones were well purified fromSalvia miltiorrhizaBunge. |
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7.
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Overcoming
matrix effects in electrospray: Quantitation of β-agonists in complex
matrices by isotope dilution liquid chromatography–mass spectrometry using
singly 13C-labeled analogues
Original Research
Article
Pages 40-47 Ana González-Antuña, Juan C. Domínguez-Romero, Juan F. García-Reyes, Pablo Rodríguez-González, Giuseppe Centineo, J. Ignacio García Alonso, Antonio Molina-Díaz
Highlights
► A novel
strategy based on isotope dilution mass spectrometry for LC–MS is proposed. ►
Significant minimization of matrix effects occurring in electrospray LC–MS. ►
Study of parameters affecting the measurement of isotope abundances by
LC–TOFMS. ► Increased accuracy and precision for ultratrace level detection
in complex matrices. ► Applied successfully to ultratrace detection of
β-agonists in urine and liver. |
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8.
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Derivatization
method for sensitive determination of fluorotelomer alcohols in sediment by
liquid chromatography–electrospray tandem mass spectrometry Original Research Article
Pages 48-53 Hui Peng, Kejun Hu, Fanrong Zhao, Jianying Hu |
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9.
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Characterization
of oxidized phospholipids in oxidatively modified low density lipoproteins by
nanoflow liquid chromatography–tandem mass spectrometry Original Research Article
Pages 54-62 Ju Yong Lee, Sangsoo Lim, Sungha Park, Myeong Hee Moon |
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10.
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Analysis
of multi-class pharmaceuticals in fish tissues by ultra-high-performance
liquid chromatography tandem mass spectrometry Original Research Article
Pages 63-72 B. Huerta, A. Jakimska, M. Gros, S. Rodríguez-Mozaz, D. Barceló |
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11.
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Evaluation
of mobile phase composition for enhancing sensitivity of targeted
quantification of oligonucleotides using ultra-high performance liquid
chromatography and mass spectrometry: Application to phosphorothioate
deoxyribonucleic acid Original Research Article
Pages 73-81 Buyun Chen, Michael G. Bartlett |
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12.
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Use
of ultra-high pressure liquid chromatography coupled to high resolution mass
spectrometry for fast screening in high throughput doping control Original Research Article
Pages 82-95 Alessandro Musenga, David A. Cowan |
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Gas Chromatography
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13.
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Determination
of adsorption isotherms of chlorinated hydrocarbons on halloysite adsorbent
by inverse gas chromatography
Original Research
Article
Pages 96-100 K. Czech, P.M. Słomkiewicz
Highlights
►
Acid-activated halloysite is active adsorbent for chlorinated hydrocarbons. ►
Two methods maximum and division peak of inverse gas chromatography are
comparable. |
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14.
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Effect
of impregnating agent and relative humidity on surface characteristics of
sorbents determined by inverse gas chromatography Original Research Article
Pages 101-104 M. Kasperkowiak, J. Kołodziejek, B. Strzemiecka, A. Voelkel
Highlights
►IGC was
applied to evaluate the surface properties of zeolite and ion-exchange
resins. ► Studied sorbents were impregnated with selected components of the
post-fermentation broth. ► Effect of various impregnating agent on the
surface properties of solids. ► Effect of different carrier gas humidity on
IGC derived surface parameters. |
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15.
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Multidimensional
gas chromatography using microfluidic switching and low thermal mass gas
chromatography for the characterization of targeted volatile organic
compounds Original Research Article
Pages 105-110 J. Luong, R. Gras, M. Hawryluk, R.A. Shellie, H.J. Cortes |
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16.
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D-optimal
experimental design coupled with parallel factor analysis 2 decomposition a
useful tool in the determination of triazines in oranges by programmed
temperature vaporization–gas chromatography–mass spectrometry when using
dispersive-solid phase extraction
Original Research
Article
Pages 111-126 A. Herrero, M.C. Ortiz, L.A. Sarabia |
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17.
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Qualitative
and quantitative analysis of vetiver essential oils by comprehensive
two-dimensional gas chromatography and comprehensive two-dimensional gas
chromatography/mass spectrometry
Original Research
Article
Pages 127-148 Jean-Jacques Filippi, Emilie Belhassen, Nicolas Baldovini, Hugues Brevard, Uwe J. Meierhenrich |
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Electrophoresis and
Electrochromatography
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18.
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Determination
of association constants between 5′-guanosine monophosphate gel and aromatic
compounds by capillary electrophoresis
Original Research
Article
Pages 149-154 Kaori Yamaguchi, Nobuyuki Takeyasu, Takashi Kaneta |
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Short Communication
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Column Liquid
Chromatography
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19.
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Selective
determination method for measurement of methylmercury and ethylmercury in
soil/sediment samples using high-performance liquid
chromatography–chemiluminescence detection coupled with simple extraction
technique
Pages 155-159 Hitoshi Kodamatani, Takashi Tomiyasu
Highlights
► A
selective determination method for MeHg+and EtHg+was developed. ► The
developed method was applied to various soil/sediment samples. ► EtHg+was
first detected from ERM CC 580 of certified reference material. ► Preliminary
study concerning a relationship between T-Hg and MeHg+was performed. |
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